Ramping method EN 17505:2023

Advanced Carbon Analysis According to EN 17505:2023

The new EN 17505:2023 standard sets forth methodologies for the accurate differentiation and measurement of total carbon (TOC), residual oxidizable carbon (ROC), and inorganic carbon (TIC) in soil and waste materials. These procedures are crucial for environmental assessments, enabling precise quantification of carbon content essential for soil fertility and pollution control.

EN 17505:2023 introduces a rigorous approach by specifying the temperature-dependent differentiation of carbon types. TOC400 is measured at 400°C, indicative of organic carbon readily oxidizable at this temperature. ROC, measurable at either 600°C or 900°C depending on the method, represents carbon forms that resist initial combustion but decompose at higher temperatures, including substances like lignite and charcoal. Lastly, TIC900 is quantified at 900°C, capturing the carbon typically found in carbonates that decompose at high temperatures to release CO2​ (BSI Group)​​ (https://www.en-standard.eu)​.

 Understanding BS EN 17505:2023 for Advanced Soil and Waste Characterization

Standard EN 17505:2023 is a pivotal European standard that specifies a robust method for differentiating total carbon in soil and waste materials through temperature-dependent analysis. This standard is crucial for laboratories and environmental agencies committed to precise soil and waste characterization, offering a detailed protocol for quantifying organic, residual oxidizable, and inorganic carbon components.

 Key Features of EN 17505:2023

The standard classifies carbon into three distinct types based on their combustion characteristics at specific temperatures:

Total Organic Carbon (TOC400): Organic carbon released at temperatures up to 400°C, which typically includes biodegradable material.

Residual Oxidizable Carbon (ROC): Carbon types such as lignite, charcoal, and soot, which resist initial combustion but oxidize at elevated temperatures, specifically measured at 600°C and 900°C depending on the method.

Total Inorganic Carbon (TIC900): Inorganic carbon, generally from carbonates, released at temperatures up to 900°C.

These measurements are performed through dry combustion in an oxygen-rich environment, with temperatures spanning from 150°C to 900°C. This process ensures that all carbon forms in the sample—whether from soil, anthropogenic mixtures, or solid waste—are accurately quantified, provided they exceed a minimal threshold of 1 g of carbon per kg of sample.

 Application Areas

EN 17505:2023 is applicable in various critical sectors:

– Solid Wastes (ICS 13.030.10): Enabling comprehensive waste characterization to manage disposal and recycling processes effectively.

– Chemical Characteristics of Soils (ICS 13.080.10): Essential for assessing soil health and fertility, impacting agricultural practices and environmental conservation efforts.


?How can you implement EN17505:2023 in your lab

For laboratories looking to implement BS EN 17505:2023, the Skalar Primacs ATC-100 system presents an optimal solution. This system not only complies with the standard but enhances the efficiency and accuracy of carbon analysis.

Unique Features of the Primacs ATC-100:

Dual Method Capability: It supports both oxidative method A and the mixed oxidative/non-oxidative method B, as specified in EN 17505:2023. Method A involves a sequential approach, placing samples at different heights within the combustion furnace to achieve the specific temperature zones required for TOC400, ROC600, and TIC900.

Method B improves the separation of carbon types by altering the carrier gas post-combustion, enhancing the precision of TIC900 measurements and subsequently re-oxidizing for ROC900 determination.

– Efficiency and Automation: Equipped with a large, integrated autosampler capable of handling up to 100 positions, the system facilitates high-throughput analysis with minimal manual intervention, crucial for busy laboratories.

– Versatile Application: Designed for diverse samples, including soil, waste, and other environmental solids, the Primacs ATC-100 is versatile across multiple analytical scenarios.

 For environmental laboratories aiming to align with the latest standards in carbon analysis, the Skalar Primacs SNC-100 is the system of choice. Its compliance with BS EN 17505:2023, combined with its advanced technological features, makes it an indispensable tool for accurate and efficient soil and waste characterization. Laboratories seeking to enhance their analytical capabilities will find the Primacs SNC-100 to be an essential addition, ensuring compliance and precision in environmental assessments. For more detailed inquiries and integration support, reaching out to Skalar is highly recommended.

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The PrimacsSN-100 presents an ideal solution for laboratories requiring swift and precise analysis of proteins across a diverse range of food and feed samples. Utilizing automation, this system significantly reduces analysis durations and amplifies sample throughput.

Ensuring utmost accuracy, our analyzers undergo rigorous testing and calibration to align with each customer's standards, guaranteeing optimal and precise results.

Key attributes of the PrimacsSN-100 include a 100-position random access autosampler with the option to prioritize samples, reusable ceramic crucibles, and capacity for sample weights up to 3g of solid material and 1g of liquid material. Its vertical sample introduction system facilitates seamless insertion of samples into the high-temperature combustion furnace, preserving sample ashes within the crucible to prevent buildup in the combustion zone and minimize maintenance time.

The determination of Total Nitrogen (TN) and protein content relies on the Dumas method and Thermal Conductivity detection (TCD), offering a rapid, safe, and eco-friendly alternative to traditional Kjeldahl methods. Pre-loaded methods cater to various sample types, including cereals, dairy, starch, grains, meats, animal feed, malt, and more.

A unique temperature ramping program is integral to the PrimacsSN-100, particularly beneficial for samples prone to erratic combustion behaviors like meat and vegetable oil. This patented technique allows for customized combustion temperature profiles tailored to specific sample matrices, ensuring optimal combustion patterns for accurate analysis.

Overall, the PrimacsSN-100 delivers fast, precise, and reliable TN/protein analysis across a spectrum of food samples, facilitating uninterrupted operation for enhanced efficiency and high-quality results.

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